EHANOL EXTRACTION AND WINTERIZATION REACTOR SYSTEM
20L Ethanol Reactor Base System 20 liter jacketed reactor base system designed specifically to operate at the extremely low temperatures required to perform ethanol extraction and winterization. Contact our technical support staff to choose a chiller with the appropriate connections, explosion proof motor and any other accessories needed
20L Ethanol Reactor Base System 20 liter jacketed reactor base system designed specifically to operate at the extremely low temperatures required to perform ethanol extraction and winterization. Contact our technical support staff to choose a chiller with the appropriate connections, explosion proof motor and any other accessories needed
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➧➧Rugged, steel-reinforced PTFE stirring rod
➧➧Heavy duty mechanical lab stirrer
➧➧Temperature controlled heating mantle
Complete reaction assembly using standard ACE reaction equipment. The 12L through 72L flasks have three 65/40 in-line spherical joints and two 29/42 standard taper joints.
Features
• Full range of pilot-size flasks from 12L to 72L with spherical and standard taper joints.
• Rugged 19mm diameter, steel-reinforced PTFE stirring rod needs no lubrication. Runs in a precision Trubore™ bearing. The PTFE paddle is removable, and other interchangeable agitators available from ACE may be substituted.
• The 12L assembly has a 10mm diameter steel-reinforced PTFE rod, as well as a 10mm bearing, chuck, and paddle.
• Highly efficient 6016 condenser is attached directly to 65/40 side joint.
• Thermowell depth is completely adjustable via an Ace‑Thred adapter.
• Unit as supplied has a heavy-duty mechanical lab stirrer; for situations that call for nonelectric motors, ACE can supply a compact air-driven motor and support. Call or e-mail for a quotation.
• Heavy-duty bottom heating mantle.
• Approximate overall height: 12L and 22L – 59”; 50L and 72L – 63”
ACE heavy wall borosilicate glass Pressure Reactors have been designed and tested to provide the chemist with a system to perform low to moderate positive pressure reactions, synthesis, and catalysis; or simply to run reactions under inert gas conditions. Reactor capacities range from 500mL to 5000mL, and use Ace‑Threds to achieve a leak-tight system.
Two types of Pressure Reactors are available:
- 1— Two-Piece System, with a maximum pressure limit of 35psig @ 100°C
- 2— One-Piece System, with a maximum pressure limit of 45psig @ 100°C
The Two-Piece System consists of a flanged flask and head with a shallow O‑Ring groove, O‑Ring, and quickrelease clamp. Flange sizes range from 60mm to 150mm inside diameter, allowing the use of large agitators and facilitating product removal and clean-out. Both systems offer jacketed and unjacketed vessels, with or without bottom outlet valves. These jackets are heat-sealed.
Complete systems and their components are listed on the following pages. Systems are available with:
- Liquid addition funnel
- Solid addition funnel
- Stirring motor, controller and flexible shaft
- Heating mantle and temperature control system
- Thermowell
- Moisture test receiver
- Temperature controller with thermocouple
- Pressure relief manifold
- Support Stands
PHOTOBIOLOGICAL-OXIDATION APPARATUS 1200W, U.V., Flow-Thru
Modified version of 7900 Apparatus. Sample tubes have been replaced with a flow-thru quartz or borosilicate coil for continuous radiation of small (as little as 175mL) or large samples. Coil is available with cooling jacket for slow flow rates or without jacket when heating of sample is not a concern because of the higher flow rate.
Apparatus consists of a cylindrical lamp housing, medium pressure 1200 watt photochemical lamp, quartz or borosilicate glass coil (with or without jacket), and power supply. Access door is provided for set-up, inspection and repairs only — for your safety, do not use this door while the unit is in operation.
A cooling fan is located at bottom of housing for air movement. Lamp power supply includes a manual or automatic twelve-hour timer selector for programming exposure time. Available in 220v, 60Hz or 230v, 50Hz. Lamp housing measures 12” wide x 20” deep x 36” high, and weighs 75 lbs. Power supply measures 11” wide x 18” deep x 11” high, and weighs approximately 75 lbs. Coil is 12.7mm O.D. x 8.0mm (5/16”) I.D. with 1/2” Swagelok ends, 16 ±1 turns with approximate capacity of 175mL, maximum flow rate of 10L/min.
Ace Glass Scale-Up Series™ reactor systems enable the researcher to scale-up from 100mL to 6000mL on the bench and enjoy the same geometry when replicating those results in our Kilo Scale reactors. Simply select the capacity you desire in the base system seen below. Complete your system with any of the many optional components we offer.
Scale-Up Systems include:
• Single Reactor Stand
• Bolt Latch Clamp
• Support Ring
• Unjacketed Flask with O-Ring and Cla
Rugged, heavy wall reactor with 60mm, 100mm, or 150mm Duran® style top flange with O‑Ring groove at top, for connection to 6527, 6528, or 6529 heads, with 6517 quick-release clamp. Bottom has an Ace‑Thred (internal glass thread) for installing 5838-83 (#50) or 5857-86 (#80) bottom adapter with filter support and drain valve. Head has three 24/40 joints on 60mm size; four 24/40 joints on 100mm and 150mm sizes. Major Design Features
- – 100mL to 6000mL standard
- – Unjacketed or Jacketed
- -All inert materials
- -Reactions at ambient or pressure conditions
- -Filtering by vacuum and/or pressure
- -Removable/changeable filters, poly screen or glass, wide choice of porosities
- -Mechanical agitation
- -Inert bottom drain valve
- -Easy assembly/disassembly for cleaning
Universal open frame stand design allows for maximum clearance and access to the ports on the head. To allow for scale up, the frame has been designed to be fitted with vessels from 10L to 200L in size. For versatility, our systems have been designed with a working temperature range of ambient through 200˚C, and wetted surfaces of borosilicate glass and PTFE.
Unjacketed Kilo Systems include:
- • 4 Post Reactor Stand
- • Unjacketed Spherical Flask
- • Head, Coupling and O-Rings
- • Agitator, Stir Shaft, Bearing & Collar
- • Lid and Clamp
- • Bottom Drain Valve
- • Heating Mantle
- • Temperature Controller with Probe
- • Cooling/Heating Coil (not pictured)
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