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REACTION SYSTEM #50 Ace-Thred, 450W
Complete reaction assembly with all parts needed for immediate operation. Utilizes an internally threaded connection in place of the ground glass joint. Bushing and FETFE O‑Ring form a compression type seal with immersion well. Well has removable inner cooling tube. Reactor has (1) 14/20 angled joint for sparger tube, (1) 24/40 vertical joint for condenser, and (1) #7 Ace-Thred for thermometer. Volume indicated is total volume. Actual working volume is approximately 40-50% of total.
REACTION SYSTEM Standard Taper, 450W
Complete reaction assembly with all parts needed for immediate operation. Borosilicate glass reactor has a 60/40 center joint, (1) 14/20 angled joint for sparger tube, (1) 24/40 vertical joint for condenser, and (1) #7 Ace-Thred joint to accommodate thermometer. Volumes indicated are total volumes. Volume in reactive area of lamp is 40-50% of the total volume.
These heavy wall bottles are unique in that Ace- Threds allow for easy closing of plugs, which are reusable. The plugs have O-rings for assurance of a tight seal by simply hand tightening. The bottles are offered in several lengths with #7, #15, #25, or #36 Ace-Threds. They can be custom fabricated in various lengths and diameters, if needed.For pressure work, a “Front Seal” plug (5846) is recommended. “Back Seal” plugs (8545) are also available, if preferred. Bottles have a pressure rating of 60psig at room temperature.Complete items include Glass Bottle and PTFE Plug with FETFE® O-Ring. Replacement O-rings and O-rings of different compositions are available. Also available, as an option, for monitoring purposes, the bottles can be assembled with a stainless steel, 0-160psig pressure gauge using a 5844 Adapter in place of the 5845 or 5846 Plugs. Stainless steel extensions are offered to allow use of the tube in a furnace.
Round bottom pressure flask, with either #15 or #25 PTFE plug seal top opening. The 8417 product family also has a side thermowell port to facilitate a thermometer or a temperature probe to measure flask temperature without losing the pressure integrity of the vessel. The flask has a PTFE front-seal plug with FETFE O-Ring for an optimum seal. Flasks have a pressure rating of 60psig at 120°C. All flasks are tested at 1.5x for pressure rating
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Tabular Specificatios
Heavy wall tube with bushing and plunger valve that allows purging of the tube. Closed bottom plunger has a hole inside, that when positioned in relation to O-Ring seal, will open Tube to the atmosphere (i.e.,pull to close, push to open). Plunger has step-down extension that acts as stop in bushing. Complete item consists of Tube (#7 or #15 Ace-Thred), PTFE Bushing with FETFE® O-Ring, and Plunger Valve.
Ace Glass pressure tubes are the premier glass pressure tubes in the world, rated at 150psig at 120°C.Featuring a #7 Ace-Thred sample port, these tubes offer the convenience of sampling while remaining connected to the researcher’s apparatus.
PRESSURE TUBES 150psig @ 120°C These heavy wall tubes are unique in that Ace-Threds allow for easy closing of plugs, which are reusable. The plugs have O-rings for assurance of a tight seal by simply hand tightening.
The tubes are offered in several lengths with #7, #15, #25, or #36 Ace-Threds. They can be custom fabricated in various lengths and diameters, if needed.
For pressure work, a “Front Seal” plug (5846) is recommended. “Back Seal” plugs (8545) are also available, if preferred. Tubes have a pressure rating of 150psig at 120°C.
Complete items include Glass Tube and PTFE Plug with FETFE® O-Ring.
Note: Also available, as an option, for monitoring purposes, the tubes can be assembled with a stainless steel, 0-160psig pressure gauge (previous page) using a 5844 Adapter in place of the 5845 or 5846 Plugs. Stainless steel tube extensions are offered to allow use of the tube in a furnace
Ace Glass Scale-Up Series™ reactor systems enable the researcher to scale-up from 100mL to 6000mL on the bench and enjoy the same geometry when replicating those results in our Kilo Scale reactors. Simply select the capacity you desire in the base system seen below. Complete your system with any of the many optional components we offer: Scale-Up Systems include:
- Single Reactor Stand
- Bolt Latch Clamp
- Support Ring
- Jacketed Flask with O-Ring and Clamp
- Flange Clamp and Gasket
20L Ethanol Reactor Base System 20 liter jacketed reactor base system designed specifically to operate at the extremely low temperatures required to perform ethanol extraction and winterization. Contact our technical support staff to choose a chiller with the appropriate connections, explosion proof motor and any other accessories needed
PHOTOBIOLOGICAL-OXIDATION APPARATUS 1200W, U.V., Flow-Thru
Modified version of 7900 Apparatus. Sample tubes have been replaced with a flow-thru quartz or borosilicate coil for continuous radiation of small (as little as 175mL) or large samples. Coil is available with cooling jacket for slow flow rates or without jacket when heating of sample is not a concern because of the higher flow rate.
Apparatus consists of a cylindrical lamp housing, medium pressure 1200 watt photochemical lamp, quartz or borosilicate glass coil (with or without jacket), and power supply. Access door is provided for set-up, inspection and repairs only — for your safety, do not use this door while the unit is in operation.
A cooling fan is located at bottom of housing for air movement. Lamp power supply includes a manual or automatic twelve-hour timer selector for programming exposure time. Available in 220v, 60Hz or 230v, 50Hz. Lamp housing measures 12” wide x 20” deep x 36” high, and weighs 75 lbs. Power supply measures 11” wide x 18” deep x 11” high, and weighs approximately 75 lbs. Coil is 12.7mm O.D. x 8.0mm (5/16”) I.D. with 1/2” Swagelok ends, 16 ±1 turns with approximate capacity of 175mL, maximum flow rate of 10L/min.
Rugged, heavy wall reactor with 60mm, 100mm, or 150mm Duran® style top flange with O‑Ring groove at top, for connection to 6527, 6528, or 6529 heads, with 6517 quick-release clamp. Bottom has an Ace‑Thred (internal glass thread) for installing 5838-83 (#50) or 5857-86 (#80) bottom adapter with filter support and drain valve. Head has three 24/40 joints on 60mm size; four 24/40 joints on 100mm and 150mm sizes. Major Design Features
- – 100mL to 6000mL standard
- – Unjacketed or Jacketed
- -All inert materials
- -Reactions at ambient or pressure conditions
- -Filtering by vacuum and/or pressure
- -Removable/changeable filters, poly screen or glass, wide choice of porosities
- -Mechanical agitation
- -Inert bottom drain valve
- -Easy assembly/disassembly for cleaning
Rugged, heavy wall reactor with 60mm, 100mm, or 150mm Duran® style top flange with O‑Ring groove at top, for connection to 6527, 6528, or 6529 heads, with 6517 quick-release clamp. Bottom has an Ace‑Thred (internal glass thread) for installing 5838-83 (#50) or 5857-86 (#80) bottom adapter with filter support and drain valve. Head has three 24/40 joints on 60mm size; four 24/40 joints on 100mm and 150mm sizes. Major Design Features
- – 100mL to 6000mL standard
- – Unjacketed or Jacketed
- -All inert materials
- -Reactions at ambient or pressure conditions
- -Filtering by vacuum and/or pressure
- -Removable/changeable filters, poly screen or glass, wide choice of porosities
- -Mechanical agitation
- -Inert bottom drain valve
- -Easy assembly/disassembly for cleaning
Designed for maximum diversity and ease of use. A simple base system building platform which allows any reactor system to be customized using catalog or custom designed parts. Each system comes with the basic starting components required. Then, simply select the motor and accessories needed to complete the setup to meet your needs. Complete your system with any of the many optional components we offer.
Jacketed Kilo Systems include:
- Universal Reactor Stand
- Jacketed Flask
- Head with Clamps and O-Rings
- Agitator, Shaft, Bearing & Collar
- Drain Valve
- Couplings
200L Reactors w/Support Stand: Black epoxy-coated aluminum flask support plate is adjustable vertically, to allow room under flask for various outlet receptacles. Plate is supplied with three adjustable braces to hold mantle in place. Upper support brackets supplied to stabilize flask.
Unjacketed Kilo Systems include:
• 4 Post Reactor Stand
• Unjacketed Flask
• Head, Coupling and O-Rings
• Agitator, Stir Shaft, Bearing & Collar
• Lid and Clamp
• Bottom Drain Valve
• Heating Mantle
• Temperature Controller with Pr
➧➧Rugged, steel-reinforced PTFE stirring rod
➧➧Heavy duty mechanical lab stirrer
➧➧Temperature controlled heating mantle
Complete reaction assembly using standard ACE reaction equipment. The 12L through 72L flasks have three 65/40 in-line spherical joints and two 29/42 standard taper joints.
Features
• Full range of pilot-size flasks from 12L to 72L with spherical and standard taper joints.
• Rugged 19mm diameter, steel-reinforced PTFE stirring rod needs no lubrication. Runs in a precision Trubore™ bearing. The PTFE paddle is removable, and other interchangeable agitators available from ACE may be substituted.
• The 12L assembly has a 10mm diameter steel-reinforced PTFE rod, as well as a 10mm bearing, chuck, and paddle.
• Highly efficient 6016 condenser is attached directly to 65/40 side joint.
• Thermowell depth is completely adjustable via an Ace‑Thred adapter.
• Unit as supplied has a heavy-duty mechanical lab stirrer; for situations that call for nonelectric motors, ACE can supply a compact air-driven motor and support. Call or e-mail for a quotation.
• Heavy-duty bottom heating mantle.
• Approximate overall height: 12L and 22L – 59”; 50L and 72L – 63”
Universal open frame stand design allows for maximum clearance and access to the ports on the head. To allow for scale up, the frame has been designed to be fitted with vessels from 10L to 200L in size. For versatility, our systems have been designed with a working temperature range of ambient through 200˚C, and wetted surfaces of borosilicate glass and PTFE.
Unjacketed Kilo Systems include:
- • 4 Post Reactor Stand
- • Unjacketed Spherical Flask
- • Head, Coupling and O-Rings
- • Agitator, Stir Shaft, Bearing & Collar
- • Lid and Clamp
- • Bottom Drain Valve
- • Heating Mantle
- • Temperature Controller with Probe
- • Cooling/Heating Coil (not pictured)
