PRESSURE REACTORS ALL GLASS JACKETED
ACE heavy wall borosilicate glass Pressure Reactors have been designed and tested to provide the chemist with a system to perform low to moderate positive pressure reactions, synthesis, and catalysis; or simply to run reactions under inert gas conditions. Reactor capacities range from 500mL to 5000mL, and use Ace‑Threds to achieve a leak-tight system.
Two types of Pressure Reactors are available:
- 1— Two-Piece System, with a maximum pressure limit of 35psig @ 100°C
- 2— One-Piece System, with a maximum pressure limit of 45psig @ 100°C
The Two-Piece System consists of a flanged flask and head with a shallow O‑Ring groove, O‑Ring, and quickrelease clamp. Flange sizes range from 60mm to 150mm inside diameter, allowing the use of large agitators and facilitating product removal and clean-out. Both systems offer jacketed and unjacketed vessels, with or without bottom outlet valves. These jackets are heat-sealed.
Complete systems and their components are listed on the following pages. Systems are available with:
- Liquid addition funnel
- Solid addition funnel
- Stirring motor, controller and flexible shaft
- Heating mantle and temperature control system
- Thermowell
- Moisture test receiver
- Temperature controller with thermocouple
- Pressure relief manifold
- Support Stands
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PRESSURE TUBES 150psig @ 120°C These heavy wall tubes are unique in that Ace-Threds allow for easy closing of plugs, which are reusable. The plugs have O-rings for assurance of a tight seal by simply hand tightening.
The tubes are offered in several lengths with #7, #15, #25, or #36 Ace-Threds. They can be custom fabricated in various lengths and diameters, if needed.
For pressure work, a “Front Seal” plug (5846) is recommended. “Back Seal” plugs (8545) are also available, if preferred. Tubes have a pressure rating of 150psig at 120°C.
Complete items include Glass Tube and PTFE Plug with FETFE® O-Ring.
Note: Also available, as an option, for monitoring purposes, the tubes can be assembled with a stainless steel, 0-160psig pressure gauge (previous page) using a 5844 Adapter in place of the 5845 or 5846 Plugs. Stainless steel tube extensions are offered to allow use of the tube in a furnace
Heavy wall tube with bushing and plunger valve that allows purging of the tube. Closed bottom plunger has a hole inside, that when positioned in relation to O-Ring seal, will open Tube to the atmosphere (i.e.,pull to close, push to open). Plunger has step-down extension that acts as stop in bushing. Complete item consists of Tube (#7 or #15 Ace-Thred), PTFE Bushing with FETFE® O-Ring, and Plunger Valve.
These heavy wall bottles are unique in that Ace- Threds allow for easy closing of plugs, which are reusable. The plugs have O-rings for assurance of a tight seal by simply hand tightening. The bottles are offered in several lengths with #7, #15, #25, or #36 Ace-Threds. They can be custom fabricated in various lengths and diameters, if needed.For pressure work, a “Front Seal” plug (5846) is recommended. “Back Seal” plugs (8545) are also available, if preferred. Bottles have a pressure rating of 60psig at room temperature.Complete items include Glass Bottle and PTFE Plug with FETFE® O-Ring. Replacement O-rings and O-rings of different compositions are available. Also available, as an option, for monitoring purposes, the bottles can be assembled with a stainless steel, 0-160psig pressure gauge using a 5844 Adapter in place of the 5845 or 5846 Plugs. Stainless steel extensions are offered to allow use of the tube in a furnace.
Round bottom pressure flask, with either #15 or #25 PTFE plug seal top opening. The 8417 product family also has a side thermowell port to facilitate a thermometer or a temperature probe to measure flask temperature without losing the pressure integrity of the vessel. The flask has a PTFE front-seal plug with FETFE O-Ring for an optimum seal. Flasks have a pressure rating of 60psig at 120°C. All flasks are tested at 1.5x for pressure rating
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